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- W2950597943 abstract "Open-chain C-nucleosides, 1-(s-triazolo[4,3-x]azinyl-3)polyols 13–18 were prepared by one-pot synthesis from hydrazinoazines 20a,c and various D-aldoses 1–6. No protective groups were required for these transformations. 1-(s-Triazolo[4,3-b]pyridazinyl-3)-D-xylo-tetritol (15a) was isolated and characterised in the form of its 4-O-triphenylmethyl derivative 19. Reaction of hydrazinopyridazines 20a,b with methyl 2,3-di-O-acetyl-L-threuronate (22), followed by treatment with bromine, gave the corresponding (2R,3S)-2,3-diacetoxy-3-(s-triazolo[4,3-b]pyridazinyl-3)propanoic acid methyl esters 24a,b. Acetonisation of 1-(6-chloro-s-triazolo[4,3-b]pyridazinyl-3)-D-gluco-pentitol (17a) gave a mixture of isomeric bis-acetonides 25 and 26, while acetonisation of 1-(6-chloro-s-triazolo[4,3-b]pyridazinyl-3)-D-manno-pentitol (18a) gave acetonide 27 as a single isomer." @default.
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- W2950597943 date "1997-07-01" @default.
- W2950597943 modified "2023-10-15" @default.
- W2950597943 title "A simple one pot synthesis of 1-(s-triazolo[4,3-x]azinyl-3)-substituted polyols" @default.
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- W2950597943 doi "https://doi.org/10.1002/jhet.5570340404" @default.
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