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- W2950603602 abstract "The cluster compound [Mo 2 Fe 2 (μ 3 -S) 4 - (S 2 CNEt 2 ) 5 ]CH 3 CN has been prepared from the reaction system containing (NH 4 ) 2 MoS 4 , FeCl 3 , NaS 2 CNEt 2 , PhSH and NaOCH 3 . The crystal and molecular structure have been determined by the low temperature X-ray diffraction technique. The compound crystallizes in space group P 2 1 / c of the monoclinic system with a = 19.397(7), b = 10.891(7), c = 24.302(8) A, β = 108.95(2)° and Z = 4. With use of 2647 reflections ( I )>2.5σ( I )) the structure was refined to R ( R w ) = 0.045(0.036). The cluster Mo 2 Fe 2 S 4 (S 2 CNEt 2 ) 5 has a cubane-like skeleton [Mo 2 Fe 2 S 4 ] 5+ . Each metal atom is coordinated by three μ 3 -S atoms and a disulfide chelate terminal ligand. The fifth S 2 CNEt 2 group as a bridging ligand coordinates to two Mo atoms. In a molecule of the compound, the two Mo atoms are equivalent but the two Fe atoms are unequivalent." @default.
- W2950603602 created "2019-06-27" @default.
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- W2950603602 date "1990-02-13" @default.
- W2950603602 modified "2023-09-27" @default.
- W2950603602 title "ChemInform Abstract: Synthesis and Structure of a Novel Molybdenum-Iron-Sulfur Cluster with Mo2Fe2 Core and All-Disulfide Chelate Ligands, (Mo2Fe2(μ3-S)4(S2CNEt2)5)CH3CN." @default.
- W2950603602 cites W2045997612 @default.
- W2950603602 doi "https://doi.org/10.1002/chin.199007279" @default.
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