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• W2950605460 endingPage "62" @default.
• W2950605460 startingPage "56" @default.
• W2950605460 abstract "The precipitate formed by the addition of an aqueous solution of Co(NO3)2 and Al(NO3)3 to LiOH solution has been thoroughly studied as a function of the Al:(Al+Co) ratio, z, for 0 ≤ z ≤ 1, using X-ray diffraction and thermogravimetric analysis. For 0 ≤ z ≤ 0.2, the precipitate was a mixed phase of Co(OH)2 and the layered double hydroxide (LDH) Co0.8Al0.2(OH)2(NO3)0.2·nH2O. For 0.2 ≤ z ≤ 0.4 the precipitate was a single LDH phase containing both NO3− and CO32− ions to compensate the Al3+ charge. As z increases in this range, the amount of NO3− decreases and the amount of CO32− increases. For z > 0.4, the precipitate was a two phase mixture of an LDH phase and Al(OH)3. Li[Co1−zAlz]O2 samples were made from the coprecipitated products for 0 ≤ z ≤ 0.5, by calcining the coprecipitate and Li2CO3. These Li[Co1−zAlz]O2 samples were compared to samples of the same stoichiometries made by the direct solid state reaction of Co3O4, Al(OH)3, and Li2CO3. The lattice constants varied smoothly with z for the Li[Co1−zAlz]O2 samples made from the coprecipitate. The lattice constants of the solid-state samples deviate from these for z > 0.15, suggesting the Al is not uniformly incorporated for z > 0.15 in the solid-state samples. The consequences of this are discussed." @default.
• W2950605460 created "2019-06-27" @default.
• W2950605460 creator A5011977904 @default.
• W2950605460 creator A5061318018 @default.
• W2950605460 date "2008-12-03" @default.
• W2950605460 modified "2023-09-23" @default.
• W2950605460 title "Preparation of Co_1−<i>z</i>Al_<i>z</i>(OH)₂(NO₃)_<i>z</i> Layered Double Hydroxides and Li(Co_1−<i>z</i>Al_<i>z</i>)O₂" @default.
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• W2950605460 doi "https://doi.org/10.1021/cm801627t" @default.
• W2950605460 hasPublicationYear "2008" @default.
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