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- W2950663425 abstract "The absolute configuration of vibsanin F (1), one of the simplest 11-membered ring vibsane-type diterpene, was established to be 6R, 7S and 11S by asymmetric synthesis. A diastereomer (1a) with a 6S, 7S and 11S configuration was synthesized starting from myrcene by procedures featuring a Sharpless asymmetric epoxidation and a high diastereoselective eleven-membered ring formation between a π-allylpalladium complex and a β-ketoester nucleophile. Subsequent reduction of epoxide in 1a with LiAlH4 gave a diol, which was identical with that derived from vibsanin F." @default.
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- W2950663425 date "2003-08-01" @default.
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- W2950663425 title "Determination of the absolute configuration of vibsanin F by asymmetric synthesis via π-allylpalladium complex" @default.
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- W2950663425 doi "https://doi.org/10.1016/s0040-4039(03)01537-5" @default.
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