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- W2950708045 abstract "Abstract Among the various esters of 3-(4-methoxyphenyl)glycidic acid, 4-chloro-3-methylphenyl ester (±)- 3 was found to exist as a conglomerate, and could be alternately resolved into (+)- and (−)- 3 of >98% ee by a preferential crystallization procedure. Furthermore, a 1,5-benzothiazepine derivative, (+)- 6 , a significant intermediate of diltiazem, was prepared in one pot in 76% overall yield through the treatment of enantiomerically pure (−)- 3 with 2-aminothiophenol followed by a ring closing reaction." @default.
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- W2950708045 date "2010-06-19" @default.
- W2950708045 modified "2023-09-25" @default.
- W2950708045 title "ChemInform Abstract: First Practical Resolution of a 3-(4-Methoxyphenyl)glycidic Acid Ester by Preferential Crystallization and Synthesis of Diltiazem." @default.
- W2950708045 cites W2148593364 @default.
- W2950708045 doi "https://doi.org/10.1002/chin.199840095" @default.
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