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- W2950985087 abstract "5,6-Epoxyisoprostane E2 was synthesized via bromohydrination of the cyclopentene and aldol reaction of the α-bromocyclopentanone with the epoxyaldehyde. High regioselectivity in the bromohydrination was attained with recrystallized NBS and pyridine in aqueous DMSO. The enolate for the aldol reaction was generated by adding t-BuLi to the mixture of the α-bromocyclopentanone and ZnI2. This aldol protocol was applied successfully to several cyclopentanones and aldehydes." @default.
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- W2950985087 date "2014-04-24" @default.
- W2950985087 modified "2023-09-27" @default.
- W2950985087 title "Synthesis of the PMB Ether of 5,6-Epoxyisoprostane E2 through Aldol Reaction of the α-Bromocyclopentanone" @default.
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- W2950985087 doi "https://doi.org/10.1021/ol500654g" @default.
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