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- W2951007323 abstract "A novel trimeric porphyrin array in which the macrocycles are directly fused through their β-pyrrolic carbons has been prepared and investigated. These molecules feature a 7,8,17,18-tetraethylporphyrin moiety flanked on opposite sides by two tetraphenylporphyrin (TPP) moieties. The 2,3 and 12,13 β-carbon positions of the tetraethylporphyrin substructure also function as the β-carbons in the 2 and 3 positions of the two TPP macrocycles. This framework was prepared via the reaction of 2,5-bis[(N,N,N-trimethylammonium)methyl]-3,4-diethylpyrrole diiodide with the nickel(II) complex of pyrrolo[3,4-b]-5,10,15,20-tetraphenylporphyrin, which afforded a 62-π-electron 72-atom macrocycle (2) with a central free-base tetraethylporphyrin and two terminal nickel(II) TPP functionalities. The tri-free-base complex (1) was obtained by treatment of the dinickel(II) complex with sulfuric acid followed by neutralization. Crystallographic characterization of 1 (as its tetracation salt) and 2 (as its dication salt) revealed th..." @default.
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- W2951007323 date "2000-11-02" @default.
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- W2951007323 title "β-Fused Oligoporphyrins: A Novel Approach to a New Type of Extended Aromatic System" @default.
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- W2951007323 doi "https://doi.org/10.1021/ja001316+" @default.
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