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- W2951068670 abstract "Abstract Derivatives of the branched amino sugar methyl 3-amino-2,3,6-trideoxy-3-C-methyl-α-L-ribo-hexopyranoside and its 3-nitro analog were coupled with glycosyl donors of 3,4-di-O-acetyl-2,6-dideoxy-L-fucopyranose. Successful glycosylations were developed using the fucosyl bromide, activated with silver triflate, and the fucosyl oxysilane, activated with trimethylsilyl triflate. High stereoselectivities for the desired α-1,4 linkage were observed in both cases. The N-trifluoroacetamido disaccharide was deacylated and the amino group oxidized to nitro with dimethyldioxirane. An alternate route based on coupling of the fucosyl bromide with the nitro sugar methyl α-L-decilonitroside also gave the α-linked disaccharide, which is related to oligosaccharides found in the antibiotics cororubicin and arugomycin." @default.
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- W2951068670 date "2010-06-22" @default.
- W2951068670 modified "2023-09-26" @default.
- W2951068670 title "ChemInform Abstract: Synthetic Studies of the Cororubicin Oligosaccharide: Glycosylation of Branched Amino and Nitro Sugars." @default.
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- W2951068670 doi "https://doi.org/10.1002/chin.199825253" @default.
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