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• W2951092381 abstract "Two novel indium silicates, K5In3Si7O21 (1) and K4In2Si8O21 (2), have been synthesized by a flux-growth method and characterized by single-crystal X-ray diffraction. The structure of 1 consists of siebener single chains of corner-sharing SiO4 tetrahedra running along the b axis linked via corner-sharing by In2O9 face-sharing octahedral dimers and InO5 trigonal bipyramids to form a 3D framework. The structure of 2 consists of a 3D silicate framework containing 6- and 14-ring channels. InO5 square pyramids are located within the 14-ring channels sharing corners with the silicate framework. The solid-state 29Si MAS NMR spectrum of compound 1 was recorded; it shows the influence of the indium atoms in the second coordination sphere of the silicon on the chemical shift. Crystal data: 1, orthorhombic, Pna21 (No. 33), a = 12.4914(3) A, b = 16.8849(3) A, c = 10.2275(2) A, V = 2157.1(1) A3 and Z = 4; 2, monoclinic, P21/n (No. 14), a = 8.4041(3) A, b = 11.4919(4) A, c = 10.4841(3) A, beta = 90.478(2) degrees , V = 1012.5(1) A3 and Z = 2." @default.
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• W2951092381 date "2007-03-20" @default.
• W2951092381 modified "2023-09-27" @default.
• W2951092381 title "Flux Synthesis, Crystal Structures, and Solid-State NMR Spectroscopy of Two Indium Silicates Containing Varied In−O Coordination Geometries" @default.
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• W2951092381 doi "https://doi.org/10.1021/ic0700349" @default.
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