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- W2951221622 abstract "Treatment of hydroxythiol 4 with α,α-diethoxyacetophenone at room temperature yielded a mixture of epimeric S,O-acetals 6 and 7 (1:4, 92% yield), which were efficiently separated by flash chromatography. The OTBS derivatives 8 and 9 were treated with several Grignard reagents to afford carbinols 10 and 13 respectively (85–99% yield, >95% dr). After successive hydrolysis and reduction of 10 and 13 it is possible to obtain either enantiomer of diols 16 in high optical purity (>95% er)." @default.
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- W2951221622 date "2004-03-01" @default.
- W2951221622 modified "2023-10-18" @default.
- W2951221622 title "New S,O-acetals from (1R)-(−)-myrtenal as chiral auxiliaries in nucleophilic additions" @default.
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- W2951221622 doi "https://doi.org/10.1016/j.tetlet.2004.01.046" @default.
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