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- W2951285246 abstract "Two unusual compounds, 1,3a,6,6a-tetrahydro-3a,6a-bis(trifluoromethyl)-cyclopenta[c]pyrazol-3,4,5,6-tetracarboxylic acid tetramethyl ester (C16H14N2O8F6) (3) and 2-acetyl-5,7-bis(trifluoromethyl)-4-methyl-3-methoxy-2,4,6-cycloheptatrienecarboxylic acid methyl ester (C14H11F6O3) (4), were obtained from thermolysis of 3-trifluoromethyl-substituted vinyldiazocarbonyl compounds. The crystal structures of the products were determined as part of a larger comparison study on the thermal and Rh(II)-catalyzed reactions of F- and H-vinyldiazocarbonyl compounds. The resulting structures provide the first crystallographic characterization of bis(trifluoromethyl)substituted compounds of this kind. The pure compounds with all-carbon (4) and half-heterocyclic (3) skeletons are composed of a seven- and two-annulated five-membered rings in folded butterfly and envelope conformations, respectively." @default.
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- W2951285246 date "2013-12-01" @default.
- W2951285246 modified "2023-09-27" @default.
- W2951285246 title "Thermolysis of trifluoromethyl-containing vinyldiazocarbonyl compounds and X-ray crystal structure analysis of unexpected reaction products" @default.
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- W2951285246 doi "https://doi.org/10.1016/j.jfluchem.2013.07.019" @default.
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