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• W2951383693 abstract "The new monoclinic cerium borogermanate Ce6(BO4)2Ge9O22 was synthesized under high-pressure and high-temperature conditions in a Walker-type multianvil apparatus at 10.5 GPa and 1200 °C. Ce6(BO4)2Ge9O22 crystallizes with two formula units in the space group P21/n with lattice parameters a=877.0(2), b=1079.4(2), c=1079.1(2) pm, and β=95.94(3)°. As the parameter pressure favours the formation of compounds with cations possessing high coordination numbers, it was possible to produce simultaneously BO4-tetrahedra and GeO6-octahedra in one and the same borogermanate for the first time. Furthermore, the cerium atoms show high coordination numbers (C.N.: 9 and 11), and one oxygen site bridges one boron and two germanium atoms (O[3]), which is observed here for the first time. Besides a structural discussion, temperature-dependent X-ray powder diffraction data are presented, demonstrating the metastable character of this high-pressure phase." @default.
• W2951383693 created "2019-06-27" @default.
• W2951383693 creator A5056205919 @default.
• W2951383693 creator A5058693565 @default.
• W2951383693 date "2006-02-01" @default.
• W2951383693 modified "2023-10-07" @default.
• W2951383693 title "Multianvil high-pressure/high-temperature synthesis, crystal structure, and thermal behaviour of the rare-earth borogermanate Ce6(BO4)2Ge9O22" @default.
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• W2951383693 doi "https://doi.org/10.1016/j.jssc.2005.10.028" @default.
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