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• W2951398984 abstract "A C-amide-substituted O-silylated oxime, (E)-(tert-butyldimethylsiloxyimino)acetic acid N,N-dimethylamide (8b), on treatment with 2.2 equiv of BF3·OEt2, in situ generated boracyclic nitrone-type intermediate BF3·14, which underwent cycloaddition with alkenes to give 3,5-cis-isoxazolidines as the major products. The mechanism was strongly supported by isolation of the reaction intermediate 14 that was characterized by X-ray diffraction and its further reaction. This cycloaddition was successfully applied to the synthesis of syn-HPA-12 known as an inhibitor of CERT that mediates the transport of ceramide." @default.
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• W2951398984 date "2015-04-22" @default.
• W2951398984 modified "2023-10-14" @default.
• W2951398984 title "BF₃-Mediated <i>cis</i>-Selective Cycloaddition of <i>O</i>-Silyloxime with Alkenes" @default.
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• W2951398984 doi "https://doi.org/10.1021/acs.joc.5b00426" @default.
• W2951398984 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/25859817" @default.
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