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- W2951431454 abstract "Abstract KO2 oxidation of cis -4,5-dihydro-4,5-dihydroxy-3-nitropyrene, 1 gives the known lactone, 3-nitro-5H-phenanthro[4,5-bcd]pyran-5-one, 2 . Similarly the analogous 4,5-dihydrodiol, 3 , gives the known lactone, 1-nitro-5H-phenanthro[4,5-bcd]pyran-5-one, 4 .While the yield of 2 is 80%, it is only 16% for 4 . A study of the latter oxidation, relying especially on the use of HPLC, led to a change in the conditions that increased the yield of 4 from 16 to 88%. The change was to quench the reaction with H2O2 shortly after it began instead of letting it proceed, as usual, for several hours before quenching with water." @default.
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- W2951431454 date "2010-08-22" @default.
- W2951431454 modified "2023-09-26" @default.
- W2951431454 title "ChemInform Abstract: Superoxide Oxidation of 1-Nitropyrene-cis-dihydrodiols." @default.
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- W2951431454 doi "https://doi.org/10.1002/chin.199143139" @default.
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