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• W2951491892 abstract "Abstract The new charge neutral complex [Cr(tren)SbS 3 ]·H 2 O was synthesized under solvothermal conditions applying CrCl 3 ·6H 2 O, Sb 2 S 3 , and S as starting material in an aqueous tren solution (tren = tris(2‐aminoethyl)amine)). The compound crystallizes in the non‐centrosymmetric space group P2 1 2 1 2 1 with a = 8.7779(15), b = 10.7122(17), c = 15.4286(18) Å, V = 1450.8(4) Å 3 . In the structure the Cr 3+ ion is surrounded by four N atoms of the amine molecules and by two S atoms of a trigonal pyramidal [SbS 3 ] 3− group, i.e., the latter acts as a bidentate ligand. A three‐dimensional network is formed via hydrogen bonds between the complexes and water molecules. The main resonances in the Raman spectrum can be explained on the basis of calculated data. The most intense band is due to the Sb‐S stretching vibration. The thermal properties were investigated by DTA‐TG measurements. On heating [Cr(tren)SbS 3 ]·H 2 O decomposes in two distinct steps. The first step corresponds to the removal of the water molecules and the second step to the loss of the tren ligand." @default.
• W2951491892 created "2019-06-27" @default.
• W2951491892 creator A5013386968 @default.
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• W2951491892 date "2007-10-29" @default.
• W2951491892 modified "2023-10-18" @default.
• W2951491892 title "Another Example for the Ability of the Anion to act as a Bidentate Ligand: Solvothermal Synthesis, Crystal Structure, Calculated and Experimental Raman Spectra of [Cr(tren)SbS3]·H2O" @default.
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• W2951491892 doi "https://doi.org/10.1002/zaac.200700378" @default.
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