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• W2951541175 abstract "Abstract Mesocrystals have attracted more attention owing to their unique structures and properties. Nevertheless, facile and green synthesis of well‐defined mesocrystals still remains a significant challenge. Herein, one‐dimensional (1D) rodlike monoclinic scheelite phase BiVO 4 ( m BiVO 4 ) mesocrystals having superstructures orderly assembled by m BiVO 4 nanoparticle building blocks, were created via a facile solvothermal method in the glycerol (Gly)/water mixed solvent without any additives. By adjusting the dosage of Gly and pH value of the reaction system, the microstructure of BiVO 4 can be accurately regulated. The obtained samples were carefully characterized by XRD, SEM, TEM, HRTEM, BET, FTIR, PL and UV‐vis techniques. The lower pH value and the higher dosage of Gly were propitious to form rodlike m BiVO 4 mesocrystals. Of course, the kind and concentration of reaction species in the system and the assembly force were affected by the dosage of Gly and pH value. The possible formation mechanism of the BiVO 4 mesocrystals was proposed on the basis of these analyses. The optimized rodlike m BiVO 4 mesocrystal prepared with 8 mL of Gly at pH 2 exhibited the highest photocatalytic degradation activity for methylene blue (MB) under simulated sunlight irradiation, which could be attributed to its phase composition, higher surface area, stronger light absorption and 1D rodlike morphology with short L/D ratio which may increase the separation efficiency of photogenerated electrons and holes." @default.
• W2951541175 created "2019-06-27" @default.
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• W2951541175 date "2019-06-18" @default.
• W2951541175 modified "2023-10-11" @default.
• W2951541175 title "1D Rodlike <i>m</i>BiVO₄ Mesocrystals: Preparation, Formation Mechanism and Photocatalytic Performance" @default.
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• W2951541175 doi "https://doi.org/10.1002/slct.201901410" @default.
• W2951541175 hasPublicationYear "2019" @default.
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