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- W2951569170 abstract "Abstract The reaction of triphenylglycol ( S )‐ 1 with thionyl chloride leads to the cyclic sulfites 2a and 2b in a ratio of 90:10. When the mixture of diastereomers 2a/b is treated with alcohols 3 or diols 6 , enantiomerically pure ethers 5 and 7 are obtained by an unexpected S N 1‐type ring cleavage. Enantiopure triphenyloxirane ( R )‐ 10 arises under inversion of configuration upon treatment of 2a/b with sodium azide. The configuration of the major diastereomer 2a is determined by NMR spectroscopy and by conversion into the sulfoxide ( S )‐ 15 ." @default.
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- W2951569170 date "1997-06-01" @default.
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- W2951569170 title "Enantiopure Derivatives of 1,1,2-Triphenylethane-1,2-diol by Unusual Ring Opening of Its Cyclic Sulfite" @default.
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- W2951569170 doi "https://doi.org/10.1002/jlac.199719970621" @default.
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