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• W2951610071 abstract "Multinuclear 1H, 19F, and 27Al MAS (magic angle spinning) and corresponding 2D HETCOR (heteronuclear correlation) NMR spectroscopy, in combination with powder XRD measurements, provide the direct evidence for the NH4AlF4 crystalline phase, which was formed from zeolite HY dealuminated with an aqueous (NH4)2SiF6 solution at 80 °C. The NH4AlF4 crystalline phase exhibits a characteristic second-order quadrupolar-induced 27Al NMR line shape spreading from 0 to −90 ppm (in a magnetic field of 11.7 T) and two 19F resonances at −151 and −166 ppm in the 19F NMR spectrum. An 27Al quadrupolar coupling constant (CQ) of 9.5 MHz and an asymmetry parameter (η) of 0.1 were identified, for the first time, for the NH4AlF4 crystalline phase observed. On the basis of the 19F{27Al} TRAPDOR (transfer population in double resonance) NMR results, the 19F resonances at −151 and −166 ppm are therefore assigned to 19F spins associated with the fluorines in the terminal Al−F and the bridging Al−F−Al groups, respectively." @default.
• W2951610071 created "2019-06-27" @default.
• W2951610071 creator A5008263229 @default.
• W2951610071 creator A5061250358 @default.
• W2951610071 date "2006-09-09" @default.
• W2951610071 modified "2023-10-03" @default.
• W2951610071 title "Direct Solid-State NMR Spectroscopic Evidence for the NH₄AlF₄ Crystalline Phase Derived from Zeolite HY Dealuminated with Ammonium Hexafluorosilicate" @default.
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• W2951610071 doi "https://doi.org/10.1021/jp064938b" @default.
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