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• W2951694777 startingPage "1214" @default.
• W2951694777 abstract "Intercalation of decamolybdodicobaltate(III) anion ([Co2Mo10]) in a MgAl layered double hydroxide (LDH) was carried out by an anion exchange reaction using MgAl−OH LDHs (meixnerite) as precursors. The synthesis of pure and crystalline LDHs intercalated with [Co2Mo10] required trade-offs between different reaction conditions for the [Co2Mo10] anions and the LDH layers to be stable to hydrolysis reactions. In this work, these conditions for intercalation were achieved using meixnerite precursors of Al/(Mg + Al) molar ratios larger than 0.33, a reaction pH of about 4.7, and a nonaqueous medium (ethanol/water 40 vol %) at 353 K, with an exchange time of 1 h. The structure and composition of the intercalates were established by elemental analysis, powder X-ray diffraction, FTIR and Raman spectroscopies, thermal methods, rehydration experiments, SEM and TEM microscopies, and N2 adsorption/desorption studies. Gallery heights of 0.74 and 0.97 nm were observed for the [Co2Mo10] intercalated LDHs, corresponding to two different anion orientations in the interlayers. The interlayer [Co2Mo10] is stable up to 523 K and the layer structure is stable up to 573 K, even though the morphology of the intercalated materials is retained up to 773 K." @default.
• W2951694777 created "2019-06-27" @default.
• W2951694777 creator A5013413769 @default.
• W2951694777 creator A5081268666 @default.
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• W2951694777 date "2004-03-02" @default.
• W2951694777 modified "2023-10-18" @default.
• W2951694777 title "Intercalation of Decamolybdodicobaltate(III) Anion in Layered Double Hydroxides" @default.
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• W2951694777 doi "https://doi.org/10.1021/cm034853c" @default.
• W2951694777 hasPublicationYear "2004" @default.
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