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- W2951725102 abstract "One-step, catalytic synthesis of N-arylsulfonamides via the construction of N–S bonds from the direct coupling of sodium arylsulfinates with nitroarenes was realized in the presence of FeCl2 and NaHSO3 under mild conditions. In this process, stable and readily available nitroarenes were used as nitrogen sources, and NaHSO3 acted as a reductant to provide N-arylsulfonamides in good to excellent yields. A broad range of functional groups were very well-tolerated in this reaction system. In addition, mechanistic studies indicated that the N–S bond might be generated through direct coupling of nitroarene with sodium arylsulfinate prior to the reduction of nitroarenes by NaHSO3. Accordingly, a reaction mechanism involving N-aryl-N-arenesulfonylhydroxylamine as an intermediate was proposed." @default.
- W2951725102 created "2019-06-27" @default.
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- W2951725102 date "2015-08-01" @default.
- W2951725102 modified "2023-09-27" @default.
- W2951725102 title "ChemInform Abstract: Iron-Catalyzed N-Arylsulfonamide Formation Through Directly Using Nitroarenes as Nitrogen Sources." @default.
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- W2951725102 doi "https://doi.org/10.1002/chin.201534115" @default.
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