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- W2951750666 abstract "Iodoarene-mediated cyclization of N-methoxy-2-arylethane-sulfonamides with Oxone ® was carried out to form the corresponding N-methoxy-3,4-dihydro-2,1-benzothiazine-2,2-dioxides in moderate to good yields in acetonitrile. In this reaction, reactive hypervalent iodine species, i.e., [(hydroxy)(tosyloxy)iodo]arenes, were formed in situ and reacted with N-methoxy-2-arylethanesulfonamides to form the corresponding N-methoxy-3,4-dihydro-2,1-benzothiazine-2,2-dioxides in an electrophilic manner on the aromatic ring. Ion-supported PhI could be also used for the same cyclization of N-methoxy-2-arylethanesulfonamides with Oxone ® to provide N-methoxy-3,4-dihydro-2,1-benzothiazine-2,2-dioxides in good to moderte yields. However, ion-supported PhI could not be reused for the same reaction. The same iodoarene-mediated cyclization of N-methoxy-3-phenylpropanamide and N-methoxy-4-phenylbutanamide with Oxone ® was also carried out to form the corresponding N-methoxybenzolactams in moderate yields." @default.
- W2951750666 created "2019-06-27" @default.
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- W2951750666 date "2010-01-01" @default.
- W2951750666 modified "2023-10-16" @default.
- W2951750666 title "Iodoarene-Mediated Cyclization of N-Methoxy-2-arylethanesulfonamides with Oxone" @default.
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- W2951750666 doi "https://doi.org/10.3987/com-10-s(e)4" @default.
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