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• W2951784120 abstract "Allyloxy-substituted macrocyclic dibenzodicyclohexanotetraamide 2 was prepared by the following sequence. MonoBoc-protected chiral 1,2-cyclohexanediamine (3) was treated with isophthaloyl chloride followed by removal of the Boc group to form bisisophthalamide 5. Compound 5 was then treated with allyloxyphthaloyl chloride to form the macrocyclic tetraamide 2 in a 56% yield. Chiral selector 2 was converted to its ethoxydimethylsilane derivative and heated in a suspension of silica gel and toluene to form the chiral macrocycle-containing silica gel phase 1. This phase separated the enantiomers of (±)-α-methylbenzylamine and (±)-DL-α-aminobutyric acid methyl ester in a liquid chromatograph." @default.
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• W2951784120 date "1999-03-01" @default.
• W2951784120 modified "2023-10-16" @default.
• W2951784120 title "Synthesis of a chiral macrocyclic dibenzodicyclohexanotetraamide-containing stationary phase for liquid chromatography" @default.
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• W2951784120 doi "https://doi.org/10.1002/jhet.5570360209" @default.
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