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- W2951826006 abstract "We present the synthesis, characterization by DT-TGA and IR, single crystal X-ray nuclear structure at 300 K, nuclear and magnetic structure from neutron powder diffraction on a deuterated sample at 1.4 K, and magnetic properties as a function of temperature and magnetic field of Ni3(OH)2(SO4)2(H2O)2. The structure is formed of chains, parallel to the c-axis, of edge-sharing Ni(1)O6 octahedra, connected by the corners of Ni(2)O6 octahedra to form corrugated sheets along the bc-plane. The sheets are connected to one another by the sulfate groups to form the 3D network. The magnetic properties measured by ac and dc magnetization, isothermal magnetization at 2 K, and heat capacity are characterized by a transition from a paramagnet (C = 3.954 emu K/mol and θ = −31 K) to a canted antiferromagnet at TN = 29 K with an estimated canting angle of 0.2−0.3°. Deduced from powder neutron diffraction data, the magnetic structure is modeled by alternate pairs of Ni(1) within a chain having their moments pointing along ..." @default.
- W2951826006 created "2019-06-27" @default.
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- W2951826006 date "2003-12-30" @default.
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- W2951826006 title "Hydrothermal Synthesis in the System Ni(OH)2—NiSO4: Nuclear and Magnetic Structures and Magnetic Properties of Ni3(OH)2(SO4)2 (H2O)2." @default.
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- W2951826006 doi "https://doi.org/10.1002/chin.200352009" @default.
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