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- W2951844227 abstract "Electrochemical oxidation of triphenylphosphine (1) in dichloromethane containing allylsilanes (2) in an undivided cell afforded allyltriphenylphosphonium salts (3). The addition of 1 to 2 took place exclusively at the γ-position of 2 and the reaction was extended to provide a convenient method for the synthesis of cyclic phosphonium salts (3) bearing β-exo-methylene. The yields of 3 depended on the cathode material : use of a lead cathode, which has a high hydrogen overpotential, gave favorable results. Based on the results of the voltammetric study, the process of formation of 3 is suggested to involve electrophilic attack of the triphenylphosphine radical cation on 2 as the key step." @default.
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- W2951844227 date "2010-08-23" @default.
- W2951844227 modified "2023-09-27" @default.
- W2951844227 title "ChemInform Abstract: Electrochemical Oxidation of Triphenylphosphine in the Presence of Allylsilanes: Voltammetric Studies and Regioselective Preparation of Allyltriphenylphosphonium Salts." @default.
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- W2951844227 doi "https://doi.org/10.1002/chin.199119066" @default.
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