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- W2951848372 abstract "A new hydroxylammonium compound, [(NH3OH)2CuCl4], was synthesized and its crystals were grown at room temperature by slow evaporation of aqueous solutions. The crystals were characterized through powder XRD, thermogravimetry (TG), differential thermal analysis (DTA), low temperature differential scanning calorimetric (DSC) and FTIR spectra. The X-ray powder diffraction confirms the crystallinity of the compound. A fitting decomposition pattern of the compound was formulated based on the TG and thereby confirming the formation of the compound in the stoichiometric ratio. The thermal anomalies occurring in the low temperature DSC indicate successive phase transitions. The low temperature phase transitions are attributed to the ordering of [NH3OH]+ ions. While most of the phase transitions are of first order type, the one occurring at –126 °C is of second order. Two glass transitions occur when the compound was cooled between –157.9 and –136.9 °C. The characteristic vibration bands due to [NH3OH]+ and CuCl ions are observed in the IR spectra. (© 2005 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim)" @default.
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- W2951848372 date "2005-08-30" @default.
- W2951848372 modified "2023-09-26" @default.
- W2951848372 title "Synthesis and Characterization of Dihydroxylammonium Tetrachlorocuprate Dihydrate Crystals." @default.
- W2951848372 cites W1983863906 @default.
- W2951848372 doi "https://doi.org/10.1002/chin.200535027" @default.
- W2951848372 hasPublicationYear "2005" @default.
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