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- W2951884202 abstract "A chiral bis(isoxazoline) ligand (SPRIX) containing a rigid spiro skeleton was designed and synthesized via a double intramolecular nitrile oxide cycloaddition. The optically pure SPRIX greatly accelerated the Cu(acac)2-catalyzed asymmetric reaction of diisopropylzinc with cyclohexenone to give the Michael adduct with 49% ee. This is the first example of the use of an isoxazoline ligand for a transition metal-catalyzed reaction. The X-ray crystallographic analysis of the hexacoordinated copper complex of SPRIX confirmed the ligand character." @default.
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- W2951884202 date "1999-11-04" @default.
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- W2951884202 title "Design and Synthesis of the First Spiro Bis(isoxazoline) Derivatives as Asymmetric Ligands" @default.
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- W2951884202 doi "https://doi.org/10.1021/ol9902881" @default.
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