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• W2951903089 abstract "The new borate hydrate Co7B24O42(OH)2·2 H2O was synthesized under high-pressure/high-temperature conditions of 6 GPa and 880 °C in a Walker-type multianvil apparatus. The compound crystallizes in the orthorhombic space group Pbam (Z=2) with the lattice parameters a=819.0(2), b=2016.9(4), c=769.9(2) pm, V=1.2717(4) nm3, R1=0.0758, wR2=0.0836 (all data). The new structure type of Co7B24O42(OH)2·2 H2O is built up from corner-sharing BO4 tetrahedra forming corrugated layers, that are interconnected among each other by two edge-sharing BO4 tetrahedra (B2O6 units) forming Z-shaped channels. Interestingly, the here presented structure of Co7B24O42(OH)2·2 H2O is closely related to the structures of M6B22O39·H2O (M=Fe, Co), which exhibit BO4 tetrahedra in an intermediate state on the way to edge-sharing BO4 tetrahedra." @default.
• W2951903089 created "2019-06-27" @default.
• W2951903089 creator A5003289382 @default.
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• W2951903089 date "2012-01-01" @default.
• W2951903089 modified "2023-10-14" @default.
• W2951903089 title "The new high-pressure borate Co7B24O42(OH)2·2H2O—Formation of edge-sharing BO4 tetrahedra in a hydrated borate" @default.
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• W2951903089 doi "https://doi.org/10.1016/j.jssc.2011.10.028" @default.
• W2951903089 hasPublicationYear "2012" @default.
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