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- W2952003497 abstract "Abstract The title compound 1,2-di- O -acetyl-5- O -benzoyl-3-deoxy- l - erythro -pentofuranose ( 5 ), a useful precursor for the stereospecific synthesis of β- l -nucleoside analogues as potential antiviral agents, has been synthesised by a multi-step reaction sequence from l -xylose with a 38% overall yield. The preparation involved conversion of l -xylose to 1,2- O -isopropylidene-α- l -xylofuranose which, upon selective 5-O-benzoylation and subsequent radical deoxygenation, provided the protected 3-deoxy sugar derivative. Finally, cleavage of the acetonide group gave the resulting 5- O -benzoyl-3-deoxy- l - erythro -pentose which was acetylated to afford crystalline α,β- 5 ." @default.
- W2952003497 created "2019-06-27" @default.
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- W2952003497 date "2010-06-08" @default.
- W2952003497 modified "2023-09-24" @default.
- W2952003497 title "ChemInform Abstract: 1,2-Di-O-acetyl-5-O-benzoyl-3-deoxy-L-erythro-pentofuranose, a Convenient Precursor for the Stereospecific Synthesis of Nucleoside Analogues with the Unnatural β-L-Configuration." @default.
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- W2952003497 doi "https://doi.org/10.1002/chin.200018141" @default.
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