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- W2952095913 abstract "Abstract The β-alkylthio and β-phenylthio α-ethylenic aldehydes 2 , (Z)- 6 , (E)- 6 and 9 were obtained from the corresponding β-chloro α-ethylenic aldehydes, and the α-phenylthiomethylidene ketones (Z)- 13 and (E)- 13 by Peterson reaction with α,α -dimethoxycyclohexanone followed by deacetalization. Reduction (NaBH4) or addition of organolithium compounds led to-allylic alcohols which gave α-ethylenic carbonyl compounds with removal of thiol or thiophenol after treatment by acidic moist silica gel with or without mercuric chloride. The method also worked for oxygenated compounds 21 , 22 ." @default.
- W2952095913 created "2019-06-27" @default.
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- W2952095913 date "1988-11-29" @default.
- W2952095913 modified "2023-09-25" @default.
- W2952095913 title "ChemInform Abstract: Use of Moist Silica Gel for Obtaining α-Ethylenic Carbonyl Compounds from β-Alkylthio or β-Phenylthio Allylic Alcohols." @default.
- W2952095913 cites W2062235585 @default.
- W2952095913 doi "https://doi.org/10.1002/chin.198848119" @default.
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