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- W2952102719 abstract "Two bis-(6-chloropurines) bridged by conformationally restricted tethers were synthesized as potential DNA bis-intercalating agents. Reduction of 4,6-dichloro-5-nitropyrimidine (1) afforded 5-amino-4,6-dichloropyrimidine (2) which was then used as the starting material. Reaction of 2 with 4,4′-diaminodiphenylmethane (3) and bis-(4-aminophenyl) ether (4) yielded bis-[4-(N-5-amino-4-chloro-6-pyrimidyl)aminophenyl]methane (5) and bis-[4-(N-5-amino-4-chloro-6-pyrimidyl)aminophenyl] ether (6), respectively. Acid-catalyzed condensation of the above pyrimidines, 5 and 6, with triethyl orthoformate in N,N-dimethylacetamide gave bis-[4-(6-chloro-9-purinyl)phenyl]methane (7) and bis-[4-(6-chloro-9-purinyl)phenyl] ether (8). The spectral data on the new compounds will be discussed." @default.
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- W2952102719 date "1991-02-01" @default.
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- W2952102719 title "Potential DNA bis-intercalating agents. Bridged bis-(6-chloropurines) and related compounds" @default.
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- W2952102719 doi "https://doi.org/10.1002/jhet.5570280249" @default.
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