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- W2952203871 abstract "[reaction: see text](-)-Sparteine-mediated lithiation/transmetalation/substitution of N-Boc allylic amines provides anti-configured homoaldol precursors in yields of 38-85% and enantiomeric ratios of 83:17-99:1. Subsequent O-protection and hydrolysis allows access to O-protected homoaldol adducts in good yields. The absolute configurations of the homoaldol products have been assigned by calculation of optical rotations and by X-ray crystallography of derivatives. A stereochemical course of reaction for the lithiation/transmetalation/substitution sequence is proposed." @default.
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- W2952203871 date "2000-07-28" @default.
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- W2952203871 title "Highly Enantioselective Syntheses of <i>anti</i> Homoaldol Products by (−)-Sparteine-Mediated Lithiation/Transmetalation/Substitution of <i>N</i>-Boc Allylic Amines" @default.
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- W2952203871 doi "https://doi.org/10.1021/ol006186o" @default.
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