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- W2952223193 abstract "The iron(II)-catalyzed Bach reaction of tert-butoxycarbonyl azide (BocN(3)) and allyl sulfides has been extended to include propargyl sulfides, which give N-allenylsulfenimide products. Using 10 mol % dppeFeCl(2) as catalyst the reaction proceeds at 0 degrees C with a number of different propargyl sulfides in 31-73% isolated yield. The reaction is limited by product instability toward catalyst and termination of the catalytic cycle by excess BocN(3). N-Allenylsulfenimide 2b smoothly undergoes catalytic hydrogenation and a Diels-Alder reaction with cyclopentadiene." @default.
- W2952223193 created "2019-06-27" @default.
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- W2952223193 date "2003-05-10" @default.
- W2952223193 modified "2023-10-16" @default.
- W2952223193 title "Iron(II)-Catalyzed Sulfimidation and [2,3]-Sigmatropic Rearrangement of Propargyl Sulfides with <i>tert</i>-Butoxycarbonyl Azide. Access to <i>N</i>-Allenylsulfenimides" @default.
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- W2952223193 doi "https://doi.org/10.1021/jo0340410" @default.
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