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- W2952251746 abstract "ABSTRACT The reductive dialkylation of diethyl 1,4-naphthalenedicarboxylate is achieved in high yield and moderate diastereoselectivity. In liquid ammonia at −78°C, a 5.6 : 1 ratio of trans- to cis-1,4-dimethyl-1,4-naphthalenedicarboxylates is obtained. The reductive dialkylation can also be carried out under more convenient conditions in THF at room temperature with no loss in yield, but a two-fold loss in diastereoselectivity. The alternate method is also used to synthesize 1,4-dialkylated products from ethyl bromide and allyl bromide." @default.
- W2952251746 created "2019-06-27" @default.
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- W2952251746 date "2010-05-18" @default.
- W2952251746 modified "2023-09-24" @default.
- W2952251746 title "ChemInform Abstract: Room-Temperature Reductive Dialkylation of Diethyl Naphthalenedicarboxylate." @default.
- W2952251746 cites W2118895361 @default.
- W2952251746 doi "https://doi.org/10.1002/chin.200250076" @default.
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