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• W2952302145 abstract "Abstract The isotypic lithium rare‐earth oxonitridosilicates Li Ln 5 Si 4 N 10 O ( Ln = La, Pr) were synthesized at temperatures of 1200 °C in weld shut tantalum ampoules employing liquid lithium as flux. Thereby, a silicate substructure with a low degree of condensation was obtained. LiLa 5 Si 4 N 10 O crystallizes in space group P $bar{1}$ [ Z = 1, LiLa 5 Si 4 N 10 O: a = 5.7462(11), b = 6.5620(13), c = 8.3732(17) Å, α = 103.54(3), β = 107.77(3), γ = 94.30(3), wR 2 = 0.0405, 1315 data, 96 parameters]. The nitridosilicate substructure consists of loop branched dreier single‐chains of vertex sharing SiN 4 tetrahedra. Lattice energy calculations (MAPLE) and EDX measurements confirmed the electrostatic bonding interactions and the chemical compositions. The 7 Li solid‐state MAS NMR investigation is reported." @default.
• W2952302145 created "2019-06-27" @default.
• W2952302145 creator A5002043965 @default.
• W2952302145 creator A5022595225 @default.
• W2952302145 date "2011-10-20" @default.
• W2952302145 modified "2023-10-09" @default.
• W2952302145 title "LiLa₅Si₄N₁₀O and LiPr₅Si₄N₁₀O - Chain-Type Oxonitridosilicates" @default.
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• W2952302145 doi "https://doi.org/10.1002/zaac.201100381" @default.
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