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- W2952304164 abstract "[reaction: see text] A stereocontrolled approach for the preparation of the Danishefsky intermediates has been developed starting with the azaspirobicyclic ketone as a common precursor, representing a formal total synthesis of (+/-)-halichlorine and (+/-)-pinnaic acid. This approach involves the construction of the 1,7-disubstituted 6-azaspiro[4.5]decane with the proper stereochemistry established by olefin hydrogenation followed by C-methylation of the spirotricyclic lactam and the subsequent processes involving lactam ring-opening using methyl triflate and RCM to form the azaspirotricyclic quinolizidine skeleton." @default.
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- W2952304164 date "2004-02-19" @default.
- W2952304164 modified "2023-10-09" @default.
- W2952304164 title "A Formal Total Synthesis of (±)-Halichlorine and (±)-Pinnaic Acid" @default.
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- W2952304164 doi "https://doi.org/10.1021/ol0301431" @default.
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