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- W2952325811 abstract "A full account of the total synthesis of 18-demethyl-19-hydroxy-Na-demethyl-Nb-methylsuaveoline (1), the structure assigned to macrocaffrine isolated from Rauwolfia caffra, is presented. The key steps involved are an intramolecular cycloaddition reaction of the oxazole–olefin 10 and a subsequent dehydration that generated the pentacyclic pyridine derivative 14. The spectral data and specific rotation of synthetic 1 were dissimilar to those reported for a natural sample, leaving the structure of this R. caffra alkaloid undefined." @default.
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- W2952325811 date "2007-12-01" @default.
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- W2952325811 title "Total synthesis of the proposed structure of macrocaffrine" @default.
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- W2952325811 doi "https://doi.org/10.1016/j.tet.2007.10.005" @default.
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