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- W2952364467 abstract "Abstract Reaction of M′Cl 2 (bpy) 2 (M′ = Co, Ni, Mn) with (PPh 4 ) 2 MS 4 (M = Mo, W) affords MS 4 M′(bpy) 2 . Crystals of WS 4 Co(bpy) 2 , 1 2 dmf are monoclinic space group P 2 1 / n ( a = 12.458, b = 21.862, c = 10.164 A and β = 100.0°, Z = 4, R = 0.039 for 5414 independent data). The coordination geometry around the cobalt atom is octahedrally distorted with two bipyridyl groups and two sulfur atoms being cis to each other. Reaction of M′Cl 2 (bpy) 2 with [NEt 4 ] 2 [(MS 4 ) 2 M″] (M″ = Pd, Pt) gives [M′(bpy) 3 ][(MS 4 ) 2 M″]. Crystals of [Ni(bpy) 3 ][(WS 4 ) 2 Pd] are triclinic, space group P 1 ( a = 12.771, b = 14.838, c = 12.077 A, α = 72.9, β = 116.9 and γ = 96.1°, Z = 2, R = 0.042 for 3842 independent data). In the anionic species, the central palladium atom is coordinated by two chelating WS 4 2− anions leading to a distorted PdS 4 square plane moiety, the W… Pd…W core being nearly linear (173.72(6)°). Synthesis of new ruthenium complexes [WS 4 Ru(bpy) 2 ] and [WS 4 (Ru(bpy) 2 ) 2 ][PF 6 ] 2 are also reported." @default.
- W2952364467 created "2019-06-27" @default.
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- W2952364467 date "1990-07-03" @default.
- W2952364467 modified "2023-10-18" @default.
- W2952364467 title "ChemInform Abstract: Derivatives of Tetrathiometallates. Synthesis of (MS4M′(bpy)2) (M: Mo, W; M′: Co, Ni, Mn, Ru) Complexes. Structural Characterization of (Ni(bpy)3)((WS4)2Pd)." @default.
- W2952364467 cites W2076103246 @default.
- W2952364467 doi "https://doi.org/10.1002/chin.199027280" @default.
- W2952364467 hasPublicationYear "1990" @default.
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