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- W2952384080 abstract "We report here a new, atom economical annulation to 2,1-benzisoxazole scaffolds via the BF3·Et2O-catalyzed reaction of glyoxylate esters and nitrosoarenes. The developed method represents a convergent route to this compound class from previously unexplored inputs and provides a range of 2,1-benzisoxazoles in moderate to high yields under convenient conditions. Along with exploration of substrate scope, initial mechanistic investigation through 18O labeling and the synthesis of a reaction intermediate provides evidence for an unusual umpolung addition of glyoxylates to nitrosobenzenes with high O-selectivity, followed by a new type of Friedel–Crafts cyclization." @default.
- W2952384080 created "2019-06-27" @default.
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- W2952384080 date "2015-02-19" @default.
- W2952384080 modified "2023-09-27" @default.
- W2952384080 title "ChemInform Abstract: A Lewis Acid Catalyzed Annulation to 2,1-Benzisoxazoles." @default.
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- W2952384080 doi "https://doi.org/10.1002/chin.201510166" @default.
- W2952384080 hasPublicationYear "2015" @default.
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