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• W2952451967 abstract "This chapter discusses the concatenation of polarization transfer steps in one-dimensional (1-D) homonuclear chemical shift correlated experiments. It also discusses the application of the same to oligo- and polysaccharides. Simple concatenation of several coherent and/or incoherent polarization transfer mechanisms results in a unique 1-D experiment tailored for an individual spectral problem. Typical applications include circumventing the bottleneck in polarization transfer of one mechanism by the other, and isolation of overlapping spin systems. The result is a 1-D spectrum acquired with high-digital resolution and in a relatively short time. Selective pulses and chemical-shift-selective filters are used for the necessary signal selection. As this process takes place in at least two stages, the signal separation required for concatenated experiments is less stringent compared to simple selective one-dimensional (1-D) experiments. Pulsed field gradients enhance the quality of the spectra—in particular the solvent peak suppression. Although especially useful for nuclear magnetic resonance (NMR) spectroscopy of carbohydrates, the basic ideas behind these techniques are generally applicable across the whole field of high-resolution NMR spectroscopy." @default.
• W2952451967 created "2019-06-27" @default.
• W2952451967 creator A5076963127 @default.
• W2952451967 date "1997-01-01" @default.
• W2952451967 modified "2023-10-14" @default.
• W2952451967 title "Chapter 3 Concatenation of polarization transfer steps in 1D homonuclear chemical shift correlated experiments. Application to oligo- and polysaccharides" @default.
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• W2952451967 doi "https://doi.org/10.1016/s0926-4345(97)80005-3" @default.
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