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- W2952561832 abstract "2-(Methylamino)nicotinic acid was readily prepared in high yield by reacting 2-chloronicotinic acid with 40% aq MeNH2 under microwave irradiation either at 120 degrees for 2 h or at 140 degrees C for 1.5 h. Subsequently, we found that a range of 2-aminonicotinic acids could be obtained under microwave heating. The optimal reaction conditions involved the use of 3 equiv of amine, water as the solvent and heating at 200 degrees C for 2 h in the presence of diisopropylethylamine (3 equiv). (C) 2009 Elsevier Ltd. All rights reserved." @default.
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- W2952561832 date "2009-09-08" @default.
- W2952561832 modified "2023-09-24" @default.
- W2952561832 title "ChemInform Abstract: Microwave-Assisted Synthesis of 2-Aminonicotinic Acids by Reacting 2-Chloronicotinic Acid with Amines." @default.
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- W2952561832 doi "https://doi.org/10.1002/chin.200936144" @default.
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