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- W2952573480 abstract "Some alkyl allyl carbonates and an allylammonium chloride bearing (1-(butyloxy)ethyl)oxy group at the 2-position of the allyl group were synthesized and successfully transformed to oxodimethylenemethane−palladium and −platinum complexes in one step by mixing with a transition metal(0) and triphenylphosphine. On the basis of the confirmation of vinyl ether formation by 1H NMR, the generation of oxodimethylenemethane complexes was rationalized to occur through abstraction of the β-hydrogen on the acetal carbon by an alkoxide ion which was generated from the allyl carbonate upon oxidative addition of the transition metal. The palladium-catalyzed cycloaddition of the acetonylidene group to strained olefins also proceeded successfully by using these alkyl allyl carbonates." @default.
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- W2952573480 date "1996-01-01" @default.
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- W2952573480 title "One-Step Synthesis of Oxodimethylenemethane−Transition Metal Complexes and Palladium-Catalyzed Cycloaddition Reaction" @default.
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- W2952573480 doi "https://doi.org/10.1021/jo951425k" @default.
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