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- W2952603583 abstract "Abstract A new series of enantiopure oxazolidine‐thioether and thiazolidine‐alcohol ligands have been synthesized from L ‐cysteine, S ‐methyl‐ L ‐cysteine, and L ‐methionine in a straightforward manner that allows numerous structural variations to be formed. These types of ligands have not previously been used in asymmetric palladium‐catalyzed allylations and their efficacy was explored in the reaction of rac ‐1,3‐diphenyl‐2‐propenyl acetate with dimethyl malonate. The reaction proceeds in excellent yield and with good enantioselectivity. The palladium catalyst derived from N ‐benzyl‐2,2‐dimethyl‐4‐(2‐thiapropyl)oxazolidine ( 12 ) provides the allylation product in a quantitative yield and with an enantiomeric excess of 94%. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)" @default.
- W2952603583 created "2019-06-27" @default.
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- W2952603583 date "2004-06-01" @default.
- W2952603583 modified "2023-09-26" @default.
- W2952603583 title "First Generation Cysteine- and Methionine-Derived Oxazolidine and Thiazolidine Ligands for Palladium-Catalyzed Asymmetric Allylations" @default.
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- W2952603583 doi "https://doi.org/10.1002/ejoc.200300675" @default.
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