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- W2952758305 endingPage "125" @default.
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- W2952758305 abstract "The reaction of ethyl 2-(bromomethyl)acrylate (1) with chiral N-tert-butylsulfinyl aldimines 2 and indium powder in THF at 100 °C for 48 h affords, after hydrolysis, a mixture of N-tert-butylsulfinyl aminoesters 3 and α-methylene-y-butyrolactams 4. From the reaction mixture, compounds 3 were quantitatively converted to the expected butyrolactams 4 after removal of the tert-butylsulfinyl group under acidic conditions and final basic workup. The whole process takes place in high overall yields and with fairly good stereoselectivities." @default.
- W2952758305 created "2019-06-27" @default.
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- W2952758305 date "2010-01-01" @default.
- W2952758305 modified "2023-10-15" @default.
- W2952758305 title "Stereoselective Synthesis of α-Methylene-γ-butyrolactams from Ethyl 2-(Bromomethyl)acrylate and Chiral Sulfinyl Aldimines Mediated by Indium" @default.
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- W2952758305 doi "https://doi.org/10.3987/com-09-s(s)27" @default.
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