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- W2952802431 abstract "Abstracts Enantiomeric synthesis of 3′-fluoro-apionucleosides was accomplished from 1,2- O -isopropylidene d -glyceraldehyde. The key intermediate, γ,δ-unsaturated tert -fluoro ethyl ester 7 from the fluoro allylic alcohol derivative 5 was achieved via Claisen rearrangement reaction with a 90.4% enantioselectivity. The condensation of the intermediate 10 with silylated N 4 -benzoylcytosine and 6-chloropurine followed by deprotection gave the desired pyrimidine and purine apionucleosides, respectively." @default.
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- W2952802431 date "1998-05-01" @default.
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- W2952802431 title "Enantiomeric synthesis of 3′-fluoro-apionucleosides using Claisen rearrangement" @default.
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- W2952802431 doi "https://doi.org/10.1016/s0040-4039(98)00567-x" @default.
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