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- W2952804986 abstract "Abstract α, β and γ-Ga 2 O 3 have been successfully obtained in an easily scalable synthesis using aqueous solution of gallium nitrate and sodium carbonate as starting materials without any surfactant and additive. α and β-Ga 2 O 3 were obtained by calcination at 350 and 700 °С, respectively, of α-GaOOH, prepared by controlled precipitation at constant pH 6 and T = 55 °С, with 24 h of aging. Aging was necessary to fully convert the initially preciptated gel into a well-crystalline and phase-pure material. γ-Ga 2 O 3 was obtained after calcination at 500 °С of gallia gel, synthesized at constant pH 4 and T = 25 °С, without aging. These three polymorphs have a for gallia relatively high surface area: 55 m 2 /g (α-Ga 2 O 3 ), 23 m 2 /g (β-Ga 2 O 3 ) and 116 m 2 /g (γ-Ga 2 O 3 ). The combination of X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), nitrogen physisorption and thermogravimetry (TG) was employed to characterize the samples and their formation." @default.
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- W2952804986 date "2012-09-13" @default.
- W2952804986 modified "2023-09-24" @default.
- W2952804986 title "ChemInform Abstract: Synthesis and Characterization of α-, β-, and γ-Ga2O3Prepared from Aqueous Solutions by Controlled Precipitation." @default.
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- W2952804986 doi "https://doi.org/10.1002/chin.201241015" @default.
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