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- W2952837377 abstract "- The suitably protected precursors for direct fluorination, N b -Boc di-protected 5-fluorotryptamine (13), N b -acetyl-N b -Boc protected 5-halotryptamines (15a-c), were treated with Selectfluor™ in MeCN/water in the presence of NaHCO 3 to give the corresponding 3-fluorooxindoles 14 and 16a-c in good yields. Removal of the protecting groups of 14 and 16a-c produced (3,5-difluorooxindol-3-yl)ethylamine (8) and N-acetyl-(3-fluoro-5-halooxindol-3-yl)ethylamines (9a-c) in excellent yields, respectively. These compounds are potentially non-epimerizable analogs for the putative metabolites of 5-fluorotryptamine (6) and N b -acetyl-5-halotryptamines (7a-c)." @default.
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- W2952837377 date "2009-01-01" @default.
- W2952837377 modified "2023-10-16" @default.
- W2952837377 title "Synthetic Studies on the Fluorinated Analogs for the Putative Oxindole-Type Metabolites of 5-Halotryptamines" @default.
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- W2952837377 doi "https://doi.org/10.3987/com-08-s(d)70" @default.
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