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• W2952848976 abstract "Efficient access to enantioenriched δ,δ-disubstituted δ-valerolactones is described. A soft Lewis acid/hard Brønsted base cooperative catalyst allowed for direct catalytic asymmetric γ-addition of allyl cyanide to ketones, producing tertiary homoallylic alcohols with a Z-configured α,β-unsaturated nitrile. Electrophilic activation of the nitrile functionality triggered 6-exo-dig cyclization, and subsequent N-acylation gave rise to the δ-valerolactone skeleton via CN bond cleavage." @default.
• W2952848976 created "2019-06-27" @default.
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• W2952848976 date "2014-05-01" @default.
• W2952848976 modified "2023-10-16" @default.
• W2952848976 title "Concise enantioselective synthesis of δ,δ-disubstituted δ-valerolactones" @default.
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• W2952848976 doi "https://doi.org/10.1016/j.tetlet.2014.04.006" @default.
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