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- W2952893275 abstract "The 6-cobalt-substituted [{Co3(B-β-SiW9O33(OH))(B-β-SiW8O29(OH)2)}2]22- (1) has been characterized by IR and UV−vis spectroscopy, elemental analysis, magnetic studies, electrochemistry, and gel filtration chromatography. A single-crystal X-ray analysis was carried out on K10Na12[{Co3(B-β-SiW9O33(OH))(B-β-SiW8O29(OH)2)}2]·49H2O (KNa-1), which crystallizes in the monoclinic system, space group P21/n, with a = 19.9466(8) A, b = 24.6607(10) A, c = 34.0978(13) A, β = 102.175(1)°, and Z = 2. Polyanion 1 represents a novel class of asymmetric sandwich-type polyanions. It contains three cobalt ions, which are encapsulated between an unprecedented (B-β-SiW9O34) fragment and a (B-β-SiW8O31) unit. Polyanion 1 is composed of two sandwich species via two Co−O−W bridges in the solid state and almost certainly in solution as well based on gel filtration chromatography. UV−visible spectroscopy and cyclic voltammetry also confirmed its stability. Two well-separated groups of waves appeared in the voltammetric pattern: th..." @default.
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- W2952893275 date "2006-03-07" @default.
- W2952893275 modified "2023-09-24" @default.
- W2952893275 title "Cobalt-Containing Silicotungstate Sandwich Dimer [{Co3(B-β-SiW9O33(OH)) (B-β-SiW8O29(OH)2)}2]22-." @default.
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- W2952893275 doi "https://doi.org/10.1002/chin.200610033" @default.
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