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- W2952910467 abstract "Single crystals of (NH(4))(4)[(UO(2))(5)(MoO(4))(7)](H(2)O)(5) have been synthesized hydrothermally using (NH(4))(6)Mo(7)O(24), (UO(2))(CH(3)COO)(2).2H(2)O, and H(2)O at 180 degrees C. The phase has been characterized by single-crystal X-ray diffraction using a merohedrally twinned single crystal: it is hexagonal, P6(1), a = 11.4067(5) A, c = 70.659(5) A, V = 7961.9(7) A(3), and Z = 6. The structure is based upon an open framework with composition [(UO(2))(5)(MoO(4))(7)](4-) that is composed of UO(7) pentagonal bipyramids that share vertexes with MoO(4) tetrahedra. The framework has large channels (effective pore size: 4.8 x 4.8 A(2)) parallel to the c axis and a system of smaller channels (effective pore size: 2.5 x 3.6 A(2)) parallel to [100], [110], [010], [110], [110], and [110]. The channels are occupied by NH(4)(+) cations and H(2)O molecules. The topological structure of the uranyl molybdate framework can be described either in terms of fundamental chains of UO(7) pentagonal bipyramids and MoO(4) tetrahedra or in terms of tubular building units parallel to the c axis." @default.
- W2952910467 created "2019-06-27" @default.
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- W2952910467 date "2003-03-14" @default.
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- W2952910467 title "A Novel Open Framework Uranyl Molybdate: Synthesis and Structure of (NH<sub>4</sub>)<sub>4</sub>[(UO<sub>2</sub>)<sub>5</sub>(MoO<sub>4</sub>)<sub>7</sub>](H<sub>2</sub>O)<sub>5</sub>" @default.
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- W2952910467 doi "https://doi.org/10.1021/ic020516e" @default.
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