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- W2953009561 abstract "Several approaches for the synthesis of the title compound 1 were investigated. Treatment of the ethane-1,2-diamine derivative 2 with phosphoryl chloride afforded 3-chloro-5,5-dimethylcyclohex-2-enone (3) and 1-(5,5-dimethyl-3-oxocyclohex-1-enyl)-4,5-dihydro-2-phenylimidazole (4), The reaction of 2-benzoyl-dimedone (5) with an equimolar amount of ethane-1,2-diamine led to the 2:1 adduct 6, whereas with an excess of ethane-1,2-diamine, 4,5-dihydro-2-phenylimidazole (7) and dimedone were obtained. The synthesis of the title compound 1 was achieved by reacting 2-benzoyl-3-chloro-5,5-dimethylcyclohex-2-enone (8) with ethane-1,2-diamine." @default.
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- W2953009561 date "1995-03-01" @default.
- W2953009561 modified "2023-09-27" @default.
- W2953009561 title "2,3,6,7,8,9-hexahydro-8,8-dimethyl-5-phenyl-1-<i>H</i>1,4-benzodiazepin-6-one" @default.
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- W2953009561 doi "https://doi.org/10.1002/jhet.5570320246" @default.
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